Deliverables
A brief description of the shaping techniques developed in the projects, their main drawbacks and potentials
Conditions for optimal drying process for MOF synthesis by spray-dryingThe report describe briefly the spray drying process forMOF synthesis, the conditions used and the main characteristica of the products formed
Description of shaping processes and shaped productsBrief report on the various shaping techniques developed in the project and the main characteristica of the shaped products
Optimization of spray-drying processes for high yield production of divalent MOFsA document describing briefly the spray drying process and the ways to optimize this towards high yield and high quality of the product
NPMs specification sheets for production quality control and recommendation for useThe report describe how a specification sheet following the various NPM products can look like and which data is should contain
Report on the synthesis of second generation MOF in water and in solvent with recyclingA brief report describing the main results and material properties of NPMs produced in water and with solvent recycling
Public report on the performances on shaped materials at laboratory scaleBrief report on the performance and physical properties of a selection of the shaped bodies prepared in the project
Report on the quality control of production processes at kg-scaleA report that describes the various techniques used to obtain physical and performance information abount NPM products to check their quality
Conditions for supercritical CO2 washingThe report describes the supercritical washing technique, the conditions used and the characteristica of the wasing process as compared to conventional techniques
A workshop will be arranged the third year
Delivery of a batch of 1st generation MOF (Fe-BTC) for shaping development (WP5) – 0.5kgPhysical proof that sample has been prepared incl main characterization data
Delivery of shaped productsProof that shaped products have been produced and their main characteristica are provided
Delivery of up to 10kg of NPMs by spray-dryingProof that the needed amount of NPMs have been påroduced and its characteristica are provided
Delivery of first samples for testing (WP1), post-synthesis treatments (WP2) and shaping development (WP5) – 0.1g-1kg scaleProof that sample has been prepared incl main characterisation data
Delivery of up to 5 kg MOFs by batch synthesisProof that the needed amount of MOFs have been produced by batch synthesis and the product characteristica is provided
Delivery of first samples of porous aluminosilicate for testing in WP1Proof that samples have been prapered and delivered for further processing
Delivery of up to 100kg of NPMs by mecanosynthesisProof that the needed amout of NPMs have been produced at the main characteristica is provided
Delivery of HKUST-1 for shaping development in WP5 – 0,5kg scaleProof that sample has been prepared incl main characteristica.
Delivery of up to 0.5kg MOFs by batch synthesisProof that the needed amout of MOFs have been produced and its characteristics are provided
A report describing briefly the performance of all selected NPMs for the four applications chosen
Proof that a prototype integrating the methane storage cylinder containg MOF is provided
Communication tools have been established and communicated
Publications
Author(s):
Marta Rubio-Martinez, Ceren Avci-Camur, Aaron W. Thornton, Inhar Imaz, Daniel Maspoch, Matthew R. Hill
Published in:
Chemical Society Reviews, Issue 46/11, 2017, Page(s) 3453-3480, ISSN 0306-0012
Publisher:
Royal Society of Chemistry
DOI:
10.1039/c7cs00109f
Author(s):
Giulia P. M. Bignami, Zachary H. Davis, Daniel M. Dawson, Samuel A. Morris, Samantha E. Russell, David McKay, Richard E. Parke, Dinu Iuga, Russell E. Morris, Sharon E. Ashbrook
Published in:
Chemical Science, Issue 9/4, 2018, Page(s) 850-859, ISSN 2041-6520
Publisher:
Royal Society of Chemistry
DOI:
10.1039/C7SC04649A
Author(s):
S. Hindocha, S. Poulston
Published in:
Faraday Discussions, Issue 201, 2017, Page(s) 113-125, ISSN 1359-6640
Publisher:
Royal Society of Chemistry
DOI:
10.1039/c7fd00090a
Author(s):
Francis Meunier
Published in:
Science, Issue 358/6366, 2017, Page(s) eaao0361, ISSN 0036-8075
Publisher:
American Association for the Advancement of Science
DOI:
10.1126/science.aao0361
Author(s):
Yoldes Khabzina, David Farrusseng
Published in:
Microporous and Mesoporous Materials, Issue 265, 2018, Page(s) 143-148, ISSN 1387-1811
Publisher:
Elsevier BV
DOI:
10.1016/j.micromeso.2018.02.011
Author(s):
Yoldes Khabzina, Jeremy Dhainaut, Matthias Ahlhelm, Hans-Juergen Richter, Helge Reinsch, Norbert Stock, David Farrusseng
Published in:
Industrial & Engineering Chemistry Research, Issue 57/24, 2018, Page(s) 8200-8208, ISSN 0888-5885
Publisher:
American Chemical Society
DOI:
10.1021/acs.iecr.8b00808
Author(s):
Ceren Avci-Camur, Javier Troyano, Javier Pérez-Carvajal, Alexandre Legrand, David Farrusseng, Inhar Imaz, Daniel Maspoch
Published in:
Green Chemistry, Issue 20/4, 2018, Page(s) 873-878, ISSN 1463-9262
Publisher:
Royal Society of Chemistry
DOI:
10.1039/c7gc03132g
Author(s):
Cesare Atzori, Greig C. Shearer, Lorenzo Maschio, Bartolomeo Civalleri, Francesca Bonino, Carlo Lamberti, Stian Svelle, Karl Petter Lillerud, Silvia Bordiga
Published in:
The Journal of Physical Chemistry C, 2017, ISSN 1932-7447
Publisher:
American Chemical Society
DOI:
10.1021/acs.jpcc.7b00483
Author(s):
Alexandre Legrand, Anton Pastushenko, Vladimir Lysenko, Alain Geloen, Elsje Alessandra Quadrelli, Jerome Canivet, David Farrusseng
Published in:
ChemNanoMat, Issue 2/9, 2016, Page(s) 866-872, ISSN 2199-692X
Publisher:
Wiley-VCH Verlag GmbH & Co
DOI:
10.1002/cnma.201600124
Author(s):
J. Dhainaut, C. Avci-Camur, J. Troyano, A. Legrand, J. Canivet, I. Imaz, D. Maspoch, H. Reinsch, D. Farrusseng
Published in:
CrystEngComm, 2017, ISSN 1466-8033
Publisher:
Royal Society of Chemistry
DOI:
10.1039/C7CE00338B
Author(s):
Luis Garzón-Tovar, Sabina Rodríguez-Hermida, Inhar Imaz and Daniel Maspoch
Published in:
J. Am. Chem. soc, 2017, ISSN 0002-7863
Publisher:
American Chemical Society
DOI:
10.1021/jacs.6b11240
Author(s):
Luis Garzón-Tovar, Javier Pérez-Carvajal, Inhar Imaz, Daniel Maspoch
Published in:
Advanced Functional Materials, Issue 27/21, 2017, Page(s) 1606424, ISSN 1616-301X
Publisher:
John Wiley & Sons Ltd.
DOI:
10.1002/adfm.201606424
Author(s):
Vincent Guillerm, Luis Garzón-Tovar, Amirali Yazdi, Inhar Imaz, Jordi Juanhuix, Daniel Maspoch
Published in:
Chemistry - A European Journal, Issue 23/28, 2017, Page(s) 6829-6835, ISSN 0947-6539
Publisher:
John Wiley & Sons Ltd.
DOI:
10.1002/chem.201605507
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